Micro-World Gems & Gemology, Fall 2020, Vol. 56, No. 3

Manufactured Inclusions in Gem Materials


Manufactured floral-shaped inclusion in quartz.
Figure 1. This 47 ct cabochon was creatively carved from the back, and the hollow cavity was then filled with a yellow and red composite material to highlight the floral inclusion. Photo by Robert Weldon; courtesy of Mike Bowers.

Inclusions in gems have gained popularity as social media has exposed collectors to a wide range of gem materials with interesting inclusions. As a result, there has been an increase in artificial inclusions in natural rock crystal quartz as predicted by E. Skalwold (Summer 2016 Micro-World, pp. 201–202). Recently, the authors had the opportunity to examine several unique gems with manufactured inclusions. Microscopic examination revealed that the main methods for manufacturing inclusions were carving, assembling, dyeing, three-dimensional internal laser engraving, or a combination of these methods.

This creatively carved cavity was filled with a yellow and red composite material.
Figure 2. Tool marks from a rotary abrasive burr are clearly visible in this manufactured floral-shaped inclusion (left; field of view 9.72 mm). The cavity was subsequently filled with a yellow and red composite material consisting of sand grains and a colored binder or resin material (right; field of view 4.26 mm). Photomicrographs by Nathan Renfro; courtesy of Mike Bowers.

A 47 ct rutilated quartz cabochon exhibits an eye-catching yellow and red floral-shaped inclusion produced by creative carving and filling with a colored composite material (figure 1). Microscopic examination revealed circular marks from a rotary abrasive tool used to create the intricate cavity (figure 2, left). The cavity was subsequently filled with a yellow and red composite material of fine sand grains and a colored binder or resin (figure 2, right).

Orange and yellow resin fills fractures in this round quartz tablet.
Figure 3. This 226 ct round tablet of quartz contains an orange and yellow resin-filled fracture that convincingly imitates natural iron oxide mineral staining in quartz. Photo by Robert Weldon; courtesy of Mike Bowers.
Orange and yellow resin mimics natural iron oxide staining.
Figure 4. A fracture in this rock crystal quartz has been filled with orange and yellow resin to give the appearance of natural iron oxide staining. Trapped gas bubbles make this manufactured inclusion readily identifiable. Photomicrograph by Nathan Renfro; field of view 8.94 mm. Courtesy of Mike Bowers.

Another creatively manufactured inclusion in a quartz gem can be seen in a 226 ct round tablet containing a large fracture (figure 3). The fracture was filled with colored orange and yellow resin, which resembles natural iron oxide epigenetic staining sometimes seen in rock crystal quartz. A quick examination in the microscope revealed incomplete filling and trapped gas bubbles in the colored resin (figure 4), making the separation between this manufactured inclusion and its natural counterpart quite easy.

Assembled block of polished quartz encloses fractures filled with a green resin.
Figure 5. This 109 ct polished block of quartz has been assembled from two halves that contain numerous fractures filled with green resin. They have been glued together so that the moss-like inclusion is completely enclosed in the colorless quartz. Photo by Robert Weldon; courtesy of Mike Bowers.
Fracture network containing gas bubbles in assembled quartz are filled with green resin to resemble moss.
Figure 6. This moss-like inclusion results from a fracture network in two pieces of rock crystal quartz filled with green resin and glued together to encapsulate the inclusion. The assembly plane of the two quartz halves is clearly visible on the side of the stone (left; field of view 18.80 mm). The green resin contained trapped gas bubbles, and the fractures displayed an unnatural striated appearance suggesting they were artificially induced (right; field of view 2.59 mm). Photomicrographs by Nathan Renfro; courtesy of Mike Bowers.

Creative dyeing also produced the manufactured inclusion in a 109 ct quartz with a completely enclosed green moss-like inclusion (figure 5). This stone consists of two pieces of rock crystal quartz, each with a centralized network of fine fractures that may have been artificially induced by laser, judging from their unnatural irregular pattern and striated appearance. The fracture network in each piece was subsequently filled with a dark green resin to give the appearance of a moss-like inclusion. The two halves were then glued together with colorless cement, completely enclosing the green moss-like inclusions in water clear rock crystal quartz. This left a somewhat obvious assembly plane (figure 6, left) when examined with the microscope, as well as trapped gas bubbles in the green resin-filled areas (figure 6, right).

3D internal laser engraving created these two white stellate inclusions in quartz.
Figure 7. This 724 ct rock crystal quartz contains two manufactured inclusions induced by a 3D subsurface laser-engraving process. Photo by Robert Weldon; courtesy of Mike Bowers.
3D internal laser engraving represents the latest advancement in manufactured inclusions.
Figure 8. These stellate inclusions result from 3D subsurface laser engraving, which creates light scattering micro-fractures in a controlled pattern. These represent the latest advancement in manufactured inclusions within gem materials. Photomicrograph by Nathan Renfro; field of view 23.50 mm. Courtesy of Mike Bowers.

The fourth example of manufactured inclusions recently examined is a 724 ct quartz crystal with a polished face that contains two white stellate inclusions consisting of numerous radial arms surrounding a spherical core structure (figure 7). Closer examination revealed a carefully layered series of micro-fractures consistent with 3D subsurface laser engraving (figure 8). This is by far the most technologically advanced example of a manufactured inclusion in a gem material examined by author NR.

While these four examples of manufactured inclusions may not be quite as sought after as gems with natural inclusions, they certainly can be appreciated for the efforts and techniques employed by the manufacturers. Obviously, collectors of gems that feature inclusions should be aware that manufactured inclusions such as those described here exist in the trade. While some manufactured inclusions may be intended purely as an artistic enhancement, others may be produced with the intention to deceive the consumer, and caution should be used if a manufactured origin is suspected.

Nathan Renfro is manager of colored stone identification, and Robert Weldon is director of Richard T. Liddicoat Gemological Library and Information Center, at GIA in Carlsbad, California.